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Artifact formation due to ethyl thio-incorporation into silylated steroid structures as determined in doping analysis

Author
VAN DE KERKHOF, D. H1 ; VAN OOIJEN, R. D1 ; DE BOER, D2 ; FOKKENS, R. H3 ; NIBBERING, N. M. M4 ; ZWIKKER, J. W5 ; THIJSSEN, J. H. H1 ; MAES, R. A. A1
[1] Department of Human Toxicology, Utrecht Institute of Pharmaceutical Sciences (UIPS), University of Utrecht, Sorbonnelaan 16, 3584 CA Utrecht, Netherlands
[2] Laboratório de Análises de Dopagem e Bioquímica, Instituto Nacional do Desporto, Av, Prof. Egas Moniz (Estádio Universitário), 1600-190 Lisbon, Portugal
[3] Laboratory of Supramolecular Chemistry and Technology and MESA'Research Institute, University of Twente, Enschede, Netherlands
[4] Laser Centre and Chemistry Department, Vrije Universiteit, Amsterdam, Netherlands
[5] Department of Physical Organic Chemistry, Debye Institute, Utrecht University, Utrecht, Netherlands
Source

Journal of chromatography. 2002, Vol 954, Num 1-2, pp 199-206 ; ref : 5 ref

CODEN
JOCRAM
ISSN
0021-9673
Scientific domain
Biochemistry, molecular biology, biophysics; Analytical chemistry; Pharmacology drugs
Publisher
Elsevier, Amsterdam
Publication country
Netherlands
Document type
Article
Language
English
Keyword (fr)
Ammonium Iodure Anabolisant Analyse chimique Analyse quantitative Analyse trace Androgène Androstérone Artefact Chromatographie phase gazeuse Dopage Dépistage Dérivatisation Epitestostérone Etiocholanolone Impact électron Liquide biologique Méthode couplée Préparation échantillon Silylation Spectrométrie masse Stéroïde Testostérone Urine Acétamide(N-méthyl trifluoro N-triméthylsilyl) Ethanethiol
Keyword (en)
Ammonium Iodides Anabolic agent Chemical analysis Quantitative analysis Trace analysis Androgen Androsterone Artefact Gas chromatography Doping Medical screening Derivatization Epitestosterone Etiocholanolone Electron impact Biological fluid Coupled method Sample preparation Silylation Mass spectrometry Steroid Testosterone Urine
Keyword (es)
Amonio Ioduro Agente anabólico Análisis químico Análisis cuantitativo Análisis huella Andrógeno Androsterona Artefacto Cromatografía fase gaseosa Doping Descubrimiento Derivatisación Epitestosterona Etioquolanolona Impacto electrón Líquido biológico Método acoplado Preparación muestreo Sililación Espectrometría masa Esteroide Testosterona Orina
Classification
Pascal
002 Biological and medical sciences / 002B Medical sciences / 002B02 Pharmacology. Drug treatments / 002B02A General pharmacology / 002B02A02 Analysis

Discipline
General pharmacology
Origin
Inist-CNRS
Database
PASCAL
INIST identifier
13613753

Sauf mention contraire ci-dessus, le contenu de cette notice bibliographique peut être utilisé dans le cadre d’une licence CC BY 4.0 Inist-CNRS / Unless otherwise stated above, the content of this bibliographic record may be used under a CC BY 4.0 licence by Inist-CNRS / A menos que se haya señalado antes, el contenido de este registro bibliográfico puede ser utilizado al amparo de una licencia CC BY 4.0 Inist-CNRS

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