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A screening method for the detection of synthetic glucocorticosteroids in human urine by liquid chromatography-mass spectrometry based on class-characteristic fragmentation pathways

Author
MAZZARINO, Monica1 ; TURI, Stefania1 ; BOTRE, Francesco2
[1] Federazione Medico Sportiva Italiana, Laboratorio Antidoping, Largo Giulio Onesti, 1, 00197 Rome, Italy
[2] Dipartimento per le Tecnologie, le Risorse e lo Sviluppo, Università La Sapienza, Via del Castro Laurenziano 9, 00161 Rome, Italy
Source

Analytical and bioanalytical chemistry. 2008, Vol 390, Num 5, pp 1389-1402, 14 p ; ref : 22 ref

ISSNNV
1618-2642
Scientific domain
Food science technology; Analytical chemistry; Chemistry
Publisher
Springer, Heidelberg
Publication country
Germany
Document type
Article
Language
English
Author keyword
Anti-doping analysis Glucocorticosteroids LC/MS-MS Precursor ion scan; Structure-activity relationships
Keyword (fr)
Chromatographie phase liquide Dopage Electrospray Enrichissement chimique Extraction liquide liquide Fragmentation Homme Hydrolyse enzymatique Ionisation chimique Limite détection Monitorage Précurseur Spectrométrie masse tandem Spectrométrie masse Structure moléculaire Urine Vaporisation
Keyword (en)
Liquid chromatography Doping Electrospray Chemical enrichment Liquid liquid extraction Fragmentation Human Enzymatic hydrolysis Chemical ionization Detection limit Monitoring Precursor Mass spectrometry MS/MS Mass spectrometry Molecular structure Urine Vaporization
Keyword (es)
Cromatografía fase líquida Doping Electrospray Enriquecimiento químico Extracción líquido líquido Fragmentación Hombre Ionización química Límite detección Monitoreo Precursor Espectrometría masa en tándem Espectrometría masa Estructura molecular Orina Vaporización
Classification
Pascal
001 Exact sciences and technology / 001C Chemistry / 001C04 Analytical chemistry / 001C04B Chromatographic methods and physical methods associated with chromatography / 001C04B02 Other chromatographic methods

Pascal
001 Exact sciences and technology / 001C Chemistry / 001C04 Analytical chemistry / 001C04C Spectrometric and optical methods

Discipline
Analytical chemistry
Origin
Inist-CNRS
Database
PASCAL
INIST identifier
20148651

Sauf mention contraire ci-dessus, le contenu de cette notice bibliographique peut être utilisé dans le cadre d’une licence CC BY 4.0 Inist-CNRS / Unless otherwise stated above, the content of this bibliographic record may be used under a CC BY 4.0 licence by Inist-CNRS / A menos que se haya señalado antes, el contenido de este registro bibliográfico puede ser utilizado al amparo de una licencia CC BY 4.0 Inist-CNRS

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