Solid-Phase Synthesis of α-Glucosamine Sulfoforms with Fragmentation Analysis by Tandem Mass Spectrometry
- Author
- RUNHUI LIU1 ; CHANTHAMONTRI, Chamnongsak1 ; HONGLING HAN1 ; HERNANDEZ-TORRES, Jesus M1 ; WOOD, Karl V1 ; MCLUCKEY, Scott A1 ; WEI, Alexander1
[1] Department of Chemistry, Purdue University, 560 Oval Drive, West Lafayette, Indiana 47907-2084, United States - Source
Journal of organic chemistry. 2008, Vol 73, Num 16, pp 6059-6072, 14 p
- CODEN
- JOCEAH
- ISSN
- 0022-3263
- Scientific domain
- Biochemistry, molecular biology, biophysics; Organic chemistry
- Publisher
- American Chemical Society, Washington, DC
- Publication country
- United States
- Document type
- Article
- Language
- English
- Keyword (fr)
- Acide Lewis Chromatographie HPLC Chromatographie phase liquide Composé benzylique Constante dissociation Corrélation Déprotection Déterminant antigénique Electrospray Ether Fragmentation Glucosamine Groupe hydroxyle Immobilisation Milieu acide Ose amine Phase solide Protection Régiosélectivité Schéma fragmentation Spectrométrie IR Spectrométrie Raman Spectrométrie masse tandem Stabilité Structure moléculaire Sulfate organique Sulfonation Synthèse chimique
- Keyword (en)
- Lewis acid HPLC chromatography Liquid chromatography Benzylic compound Dissociation constant Correlation Deprotection Antigenic determinant Electrospray Ether Fragmentation Glucosamine Hydroxyl group Immobilization Acid medium Aminosugar Solid phase Protection Regioselectivity Fragmentation pattern Infrared spectrometry Raman spectrometry Mass spectrometry MS/MS Stability Molecular structure Organic sulfate Sulfonation Chemical synthesis
- Keyword (es)
- Acido Lewis Cromatografía HPLC Cromatografía fase líquida Compuesto benzílico Constante disociación Correlación Desprotección Determinante antigénico Electrospray Eter Fragmentación Glucosamina Grupo hidróxilo Inmovilización Medio ácido Aminoazúcar Fase sólida Protección Regioselectividad Esquema fragmentación Espectrometría IR Espectrometría Raman Espectrometría masa en tándem Estabilidad Estructura molecular Sulfato orgánico Sulfonación Síntesis química
- Classification
- Pascal
- 001 Exact sciences and technology / 001C Chemistry / 001C03 Organic chemistry / 001C03C Preparations and properties / 001C03C07 Carbohydrates. Nucleosides and nucleotides / 001C03C07A Carbohydrates with 4, 5, 6, ... C atoms, dissacharides and oligosaccharides
- Discipline
- Organic chemistry
- Origin
- Inist-CNRS
- Database
- PASCAL
- INIST identifier
- 20561113
Sauf mention contraire ci-dessus, le contenu de cette notice bibliographique peut être utilisé dans le cadre d’une licence CC BY 4.0 Inist-CNRS / Unless otherwise stated above, the content of this bibliographic record may be used under a CC BY 4.0 licence by Inist-CNRS / A menos que se haya señalado antes, el contenido de este registro bibliográfico puede ser utilizado al amparo de una licencia CC BY 4.0 Inist-CNRS
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DOI
10.1021/jo800713m 
https://dx.doi.org/10.1021/jo800713m
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