First application of hexaaquaaluminium(III) tetrafluoroborate as a mild, recyclable, non-hygroscopic acid catalyst in organic synthesis: a simple and efficient protocol for the multigram scale synthesis of 3,4-dihydropyrimidinones by Biginelli reaction
- Author
- LITVIC, Mladen1 ; VECENAJ, Ivana1 ; MIKULDAS LADISIC, Zrinka1 ; LOVRIC, Marija1 ; VINKOVIC, Vladimir2 ; FILIPAN-LITVIC, Mirela1
[1] BELUPO Pharmaceuticals, Inc., R&D, Danica 5, 48 000 Koprivnica, Croatia
[2] Institute Ruder Bošković, Bijenička c. 54, 10002 Zagreb, Croatia - Source
Tetrahedron (Oxford. Print). 2010, Vol 66, Num 19 ; 3390, 3463-3471 [10 p.] ; ref : 71 ref
- CODEN
- TETRAB
- ISSN
- 0040-4020
- Scientific domain
- Organic chemistry
- Publisher
- Elsevier, Kidlington
- Publication country
- United Kingdom
- Document type
- Article
- Language
- English
- Author keyword
- 3,4-Dihydropyrimidinone Biginelli reaction Condensation Heterocycles Hexaaquaaluminium(III) tetrafluoroborate
- Keyword (fr)
- Acide crotonique Acide tétrafluoroborique Activité catalytique Acétoacétique acide ester Acétonitrile Aldéhyde Aluminium III Complexe Catalyseur Complexe aqua Condensation chimique Cétoester Dérivé de la pyrimidinone Dérivé du furane Dérivé du thiophène Eau Encombrement stérique Ester Hétérocycle azote Hétérocycle oxygène Hétérocycle soufre Mécanisme réaction Recyclage Réaction catalytique Synthèse chimique Synthèse organique Tétrafluoroborate Urées Aluminium(tripropanolate) Echelle multigrammes Propan-2-ol Réaction Biginelli Réaction multicomposants
- Keyword (en)
- Crotonic acid Tetrafluoboric acid Catalyst activity Acetoacetic acid esters Acetonitrile Aldehyde Aluminium III Complexes Catalyst Aqua complex Condensation reaction Ketoester Pyrimidone derivatives Furan derivatives Thiophene derivatives Water Steric hindrance Ester Nitrogen heterocycle Oxygen heterocycle Sulfur heterocycle Reaction mechanism Recycling Catalytic reaction Chemical synthesis Organic synthesis Tetrafluoborates Ureas Biginelli reaction Multicomponent reaction
- Keyword (es)
- Tetrafluorobórico ácido Actividad catalítica Acetonitrilo Aldehído Aluminio III Complejo Catalizador Complejo aqua Condensación química Cetoester Furano derivado Tiofeno derivado Agua Embarazo estérico Ester Heterociclo nitrógeno Heterociclo oxígeno Heterociclo azufre Mecanismo reacción Reconversión Reacción catalítica Síntesis química Síntesis orgánica Tetrafluoroborato Ureas
- Classification
- Pascal
- 001 Exact sciences and technology / 001C Chemistry / 001C01 General and physical chemistry / 001C01A Theory of reactions, general kinetics. Catalysis. Nomenclature, chemical documentation, computer chemistry / 001C01A03 Catalysis / 001C01A03A Catalysts: preparations and properties
- Pascal
- 001 Exact sciences and technology / 001C Chemistry / 001C03 Organic chemistry / 001C03B Reactivity and mechanisms / 001C03B02 Kinetics and mechanisms
- Pascal
- 001 Exact sciences and technology / 001C Chemistry / 001C03 Organic chemistry / 001C03C Preparations and properties / 001C03C06 Heterocyclic compounds / 001C03C06A Heterocyclic compounds with o, s, se, te hetero atom and condensed derivatives
- Pascal
- 001 Exact sciences and technology / 001C Chemistry / 001C03 Organic chemistry / 001C03C Preparations and properties / 001C03C06 Heterocyclic compounds / 001C03C06C Heterocyclic compounds with several n hetero atoms in the same ring, in separated rings or in fused rings
- Discipline
- General chemistry and physical chemistry Organic chemistry
- Origin
- Inist-CNRS
- Database
- PASCAL
- INIST identifier
- 22689918
Sauf mention contraire ci-dessus, le contenu de cette notice bibliographique peut être utilisé dans le cadre d’une licence CC BY 4.0 Inist-CNRS / Unless otherwise stated above, the content of this bibliographic record may be used under a CC BY 4.0 licence by Inist-CNRS / A menos que se haya señalado antes, el contenido de este registro bibliográfico puede ser utilizado al amparo de una licencia CC BY 4.0 Inist-CNRS
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DOI
10.1016/j.tet.2010.03.024 
https://dx.doi.org/10.1016/j.tet.2010.03.024
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